Original document(5 pages)  中文版
    The present invention is the process of setting up HPLC fingerprint of Pithecellobium clypearia benth and its standard fingerprint. First, Pithecellobium clypearia benth as medicine material is crushed and reflux extracted, the extracted liquid is concentrated, ethyl acetate extracted and decompress distilled to eliminate solvent, and the residue is dissolved in acetonitrile to obtain the test sample solution. Then, HPLC fingerprint of Pithecellobium clypearia benth is obtained through HPLC analysis of the test sample solution in Merck Lichrospher 100 RP-18e chromatographic column with flow phase comprising KDP solution and acetonitrile for gradient elution and detection at wavelength of 210 nm. The standard fingerprint of Pithecellobium clypearia benth is obtained through comparing the fingerprints of 22 batches of Pithecellobium clypearia benth medicine material and determining the common fingerprint characteristics.
Application Number
申请号
200610122924 Application Date
申请日
2006.10.20
Title 名称 Setting-up method of pithecollobium clypearia benth HPLC fingersprint and its standard fingerprint
Publication Number
公开号
1945311 Publication Date
公开日
2007.04.11
Approval Pub. Date Granted Pub. Date
International Classification 分类号 G01N30/02;G01N30/06;G01N1/28;G01N30/86;G01N30/60
Applicant(s) Name
申请人
Zhongshan Univ.
Address 地址
Inventor(s) Name 发明人 Su Weiwei;Tian Heng;Wang Xiaorui;Wang Yonggang;Peng Wei;Li Peibo;Wu Zhong
Attorney & Agent 代理人

  
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